フルテキストファイル
著者
Isoda, Yuta Department of Chemistry and Biotechnology, Graduate School of Engineering, Tottori University
Sasaki, Norihiko Department of Chemistry and Biotechnology, Graduate School of Engineering, Tottori University
Kitamura, Kei Department of Chemistry and Biotechnology, Graduate School of Engineering, Tottori University
Takahashi, Shuji Department of Chemistry and Biotechnology, Graduate School of Engineering, Tottori University
Manmode, Sujit Department of Chemistry and Biotechnology, Graduate School of Engineering, Tottori University
Takeda-Okuda, Naoko Department of Regional Environment, Faculty of Regional Sciences, Tottori University
田村 純一 Department of Chemistry and Biotechnology, Graduate School of Engineering, Tottori University / Department of Regional Environment, Faculty of Regional Sciences, Tottori University / Center for Research on Green Sustainable Chemistry, Faculty of Engineering, Tottori University 研究者総覧 KAKEN
野上 敏材 Department of Chemistry and Biotechnology, Graduate School of Engineering, Tottori University / Center for Research on Green Sustainable Chemistry, Faculty of Engineering, Tottori University 研究者総覧 KAKEN
伊藤 敏幸 Department of Chemistry and Biotechnology, Graduate School of Engineering, Tottori University / Center for Research on Green Sustainable Chemistry, Faculty of Engineering, Tottori University 研究者総覧 KAKEN
キーワード
automated synthesis
electrochemical oxidation
glycosylation
glucosamine
total synthesis
抄録
The total synthesis of TMG-chitotriomycin using an automated electrochemical synthesizer for the assembly of carbohydrate building blocks is demonstrated. We have successfully prepared a precursor of TMG-chitotriomycin, which is a structurally-pure tetrasaccharide with typical protecting groups, through the methodology of automated electrochemical solution-phase synthesis developed by us. The synthesis of structurally well-defined TMG-chitotriomycin has been accomplished in 10-steps from a disaccharide building block.
出版者
Beilstein-Institut
資料タイプ
学術雑誌論文
外部リンク
ISSN
18605397
掲載誌名
BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY
13
開始ページ
919
終了ページ
924
発行日
2017-05-16
出版者DOI
著者版フラグ
出版社版
著作権表記
© 2017 Isoda et al.; licensee Beilstein-Institut. This is an Open Access article under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/4.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. The license is subject to the Beilstein Journal of Organic Chemistry terms and conditions: (http://www.beilstein-journals.org/bjoc)
掲載情報
Isoda Yuta, Sasaki Norihiko, Kitamura Kei, et al. Total synthesis of TMG-chitotriomycin based on an automated electrochemical assembly of a disaccharide building block. BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY. 2017. 13. 919-924. doi:10.3762/bjoc.13.93
部局名
工学部・工学研究科
言語
英語
Web of Science Key ut
WOS:000407582000002