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Internal Standard Compounds for Quantitative Determination of Bile Acids by Gas Chromatography
https://repository.lib.tottori-u.ac.jp/records/5142
https://repository.lib.tottori-u.ac.jp/records/514210457630-313d-4a1a-92e0-636670cadab7
| 名前 / ファイル | ライセンス | アクション |
|---|---|---|
44_091-105.pdf (498.2 kB)
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| Item type | 学術雑誌論文 / Journal Article(1) | |||||
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| 公開日 | 2018-06-22 | |||||
| タイトル | ||||||
| タイトル | Internal Standard Compounds for Quantitative Determination of Bile Acids by Gas Chromatography | |||||
| 言語 | en | |||||
| 言語 | ||||||
| 言語 | eng | |||||
| キーワード | ||||||
| 主題 | bile acids | |||||
| キーワード | ||||||
| 主題 | biological sample | |||||
| キーワード | ||||||
| 主題 | gas chromatographic analysis | |||||
| キーワード | ||||||
| 主題 | internal standard compounds | |||||
| キーワード | ||||||
| 主題 | quantitative determination | |||||
| キーワード | ||||||
| 言語 | en | |||||
| 主題 | bile acids | |||||
| キーワード | ||||||
| 言語 | en | |||||
| 主題 | biological sample | |||||
| キーワード | ||||||
| 言語 | en | |||||
| 主題 | gas chromatographic analysis | |||||
| キーワード | ||||||
| 言語 | en | |||||
| 主題 | internal standard compounds | |||||
| キーワード | ||||||
| 言語 | en | |||||
| 主題 | quantitative determination | |||||
| 資源タイプ | ||||||
| 資源タイプ | journal article | |||||
| 著者 |
Yamaga, Nobuo
× Yamaga, Nobuo× Ogura, Yoshio× Yamada, Kazuo× Kohara, Hiromi× Uchida, Kiyohisa× Yamaga, Nobuo× Ogura, Yoshio× Yamada, Kazuo× Kohara, Hiromi× Uchida, Kiyohisa |
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| 著者所属 | ||||||
| 値 | Department of Biochemistry, Tottori University Faculty of Medicine | |||||
| 著者所属 | ||||||
| 値 | Department of Biochemistry, Tottori University Faculty of Medicine | |||||
| 著者所属 | ||||||
| 値 | Department of Biochemistry, Tottori University Faculty of Medicine | |||||
| 著者所属 | ||||||
| 値 | Department of Pathological Biochemistry, Tottori University Faculty of Medicine | |||||
| 著者所属 | ||||||
| 値 | The Cell Science Research Foundation | |||||
| 抄録 | ||||||
| 内容記述タイプ | Other | |||||
| 内容記述 | Gas chromatography is well recognized as a useful tool with several advantages for the analysis of bile acids as well as various compounds. In gas chromatographic analysis, bile acids in an analytical sample are subjected to a number of complicated procedures involving many steps such as extraction, fractionation, solvolysis, hydrolysis, derivatization and injection to the gas chromatograph. These procedures result in the loss of bile acids in the analytical sample. The addition of suitable internal standard compound(s) into the analytical sample prior to the extraction of bile acids is indispensable for an accurate determination of bile acids. There are two methods for the quantitative determination of bile acids in a biological sample by gas chromatography: one is the determination of total bile acid amounts in the sample. The other is the determination of bile acid amounts in each fraction after group separation of bile acids in the biological sample using an ion exchange gel column. The addition of 7β,12α-dihydroxy-5β-cholanoic acid or 7β,12β-dihydroxy-5β-cholanoic acid as an internal standard compound is useful for the former method. On the other hand, the addition of 7β,12β-dihydroxy-5β-cholanoic acid, glyco-7α,12α-dihydroxy-5β-cholanoic acid, tauro-7α,12β-dihydroxy-5β-cholanoic acid and glyco-7β,12α-dihydroxy-5β-cholanoic acid 7-sulfate is a suitable combination as internal standard compounds for the latter method. | |||||
| 書誌情報 |
Yonago Acta medica en : Yonago Acta medica 巻 44, 号 2, p. 91-105, 発行日 2001-07 |
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| 出版者 | ||||||
| 出版者 | Tottori University Faculty of Medicine | |||||
| ISSN | ||||||
| 収録物識別子タイプ | ISSN | |||||
| 収録物識別子 | 13468049 | |||||
| 書誌レコードID | ||||||
| 収録物識別子タイプ | NCID | |||||
| 収録物識別子 | AA00892882 | |||||
| 権利 | ||||||
| 権利情報 | Yonago Acta medica 編集委員会 | |||||
| 情報源 | ||||||
| 関連名称 | Yonago Acta medica. 2001, 44(2), 91-105 | |||||
| 著者版フラグ | ||||||
| 出版タイプ | VoR | |||||
